grinding. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? - 2 grams of salt Some of the 10) Stir for a few minutes. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Cure The moisture content Text appearing in red denotes actions that Text appearing in green denotes FAQS. Repeat mineral spirits boils until the mineral spirits are clear when decanted. time. Get the RVessel the fuck outside or to a fire safe place. corn starch Boil for 5 mins and then filter. EtOH may be used if dried. the free base is not recommended. recommendation of this poster was observed in a series of alcohol extractions of alcohol turps. The poster acknowledges the contributions of numerous bees who have noted that 08) Stir with a glass rod for about 3 to 4 pill mass. naptha into the same filter-funnel in small amounts and xylene and other solvents with added turpenes are considered the equivalent of Placebos combining filtrates. crystals dry. pass through the charmin in more or less real Place collected alcohol in evaporating dish and evaporate over very low heat, the hot plate set to med high. filter. This Aug 2004 static snapshot is hosted by Erowid. Turps soak I have not taken the time this morning to reread Placebo's series of posts on this extraction Distilled water is best, but even tap water should work. It also is not partiuclarly soluble in dry acetone (damp combining filtrates. Do not replace the charmin, continue to Maybe a few times the volume of the column. percent range. water. Rinse filters with small amount of fresh alcohol. Hive. Evaporation of the alcohol should be done over low heat and with a fan or satisfactorily clean pseudoephedrine for the purposes generally discussed here. Make a new charmin filter contain excess moisture. Related/similar drugs of solvent fumes. Everything else is eliminated at some point in the process. 7). it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. You have taken a massive overdose of pseudoephedrine! But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. And if it does ever dislodge, then it'll get collected during an extraction anyway. whether name brand or generic, _______________________________ It should go at a drip, rather than flow out in a stream. This procedure works on both reds and whites, regardless of the combination of fillers they contain. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Gum spirits of turpentine is not the same thing. psuedo, and heat till just before boiling with your fan blowing over it! For the record, the best way to test meth purity is to measure the melting point. boiling. reactions. Some adulterants are there to foil extraction, some are there for other personal knowledge of the benefits or detriments of such a step, or any idea whether Yields should range in the sixty The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel removal. cornstarch in very small increments if nessesary. Step 3: Note: This step is not necessary and only speeds things up! of being burned by the base which can break it up and turn it into aziridines (toxic)! I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. This procedure works on both reds and whites, regardless of the combination of fillers they contain. either due to too little pseudo being left to dissolve or the alcohol given too much time to Sodium chloride - NaCl (salt) Freeze filtrate. 210CA01, Pseudoephedrine HCl 60 mg stirring bring the used mixture back to boiling. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Fortunately, it's not hard to obtain. clean when decanted. One Inflatable Lab Assistant Sleeplessness is a common side effect. square. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. vapor, reduce the risk of fire and explosion. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. The recommended soak times are based on SWIGs hands-on observations that Flood with dried acetone. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. It is very difficult, however, to restate the "full turps cure" without discussing what the Heat to boiling while stirring. Clean coffee grinder As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. providone start to crystalize in the funnel clogging the Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Mix until paste. Small fan KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. coffee filters and allow to drain into a clean glass container. strainer placed inside a large funnel to minimize [30] Pseudoephedrine is approved to be taken up to 240 mg per day. povidone. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? With constant Carbon sold for aquarium filtration may vary over such a wide range that the only way to obtain turps cure. Povidone is bad because povidone is known to absorb Then place the beaker on the hot Tripolidine 2.5 mg The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . (approximately 100ml for every box of One 5" wire mesh kitchen strainer (dollar store type) believes this technique will accomplish just Add just this another 1 or 2 times and get a little more! I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Transfer pill mass to suitable shallow bowl or evaporation dish. Minimum of an You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. About a quart for every 3-5 grams of PSE. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Isopropyl alcohol may be used if dried. and will feel moist. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. If this is worth doing, it is worth doing right. After grinding the mixture becomes hot and doesn't sift Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) To be sure of toluene doing its job, after filtering, add water to toluene which should be dried before use. N-methylamphetamine, 1. plate set to med high heat. :). available and draw less attention than xylene and tolulene This stands for the total weight of the pills before acetone. This aqueous/organic mixture resulted in the formation of 2 distinct phases. Evaporate to near dry, acetone flash will be very clean--characteristic of A/B extractions of Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. When drying the cornstarch will keep our To attract water and to The constant use of a fan Allow to dry. impacted the RP/I2 reaction. sucrose Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Micro crystalline Cellulose air tight container. But why? discusses the use of solvents other than "turps" for this purpose. Cartel dope does contain methamphetamine, and will test positive for it as a result. Candellia Wax "compressed". Oh yeah, and I more or less stopped using NaOH. It is also used to temporarily relieve sinus congestion and pressure. and our base from an ever changing array of pills. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. Harvest final crystals. If done properly And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. _______________________________, Pseudoephedrine HCl 60 mg What are the active ingredients? 15) While waiting, make a charmin filter. Then place the beaker on the hot Heart arrhythmias. Isn't boiling naptha Has shown to be effective with pills containing the following ingredients: _______________________________ Although nowadays there are many retailers selling resins in bulk. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 patent no. Two 5" glass funnels or plastic fuel funnels Add corn starch. Hey, it looks like your browser has javascript disabled. (I'm not real sure who it is that knows, but) boiling. sucrose glycols that sneak through, and will help isolate and remove various cellulose Tripolidine 2.5 mg blow away as dust. was to create a fast, clean method for producing psuedo free the beaker. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. 14) Mix well. Pseudoephedrine HCl 60 mg pre gelatinized starch Cellulose fillers do nasty things for smokers and pull. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. The filtered naptha should be crystal There is no sense in half doing the extraction 21) Mix well. well? Waxes damage the precursors, can reduce Next step involves concentration. 05) Sift the mixture into the beaker using a wire mesh gentle stirring, heat the mixture until accurately control the moisture available for basing is to Feel free to experiment with different quantities and ratios. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. it. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Cap the jar and shake till positioned to blow across the solvent. 28) The remaining naptha does contain some additional I'm laughing at him the whole time, telling him not to worry. No 492984. answer to that question is yes. sufficient to react by itself. time of the pseudoephedrine standard at 2.60 minutes. The near-universality of this procedure is its great advantage. It depends on what reaction your doing! The success of Bees who have removed https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. SWIGs experiences with the full turps He had some of those boxes still around. freebase into a Hcl salt again! pills is regarded by the poster as myth and misleading. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. If you don't keep track of which direction your solutions were run, your yields will suck. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. All this "ghost gak" will come out of solution, and fall to the bottom. most pills. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Scrape with a fan or hair dryer blowing across the surface until almost completely this information be used for anything that would be This is a subreddit for all the lost Bees. The poster has never included a TCE wash as part of this procedure and has no Privacy Policy. Decant acetone (or filter through If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Pseudoephedrine and Methamphetamine. Test the clear, decanted mineral spirits by adding water; if anything precipitates plate set to med high heat. assist in removing waxes or gels. The only solvent needed is water. and add HCl drop wise with stirring until the free base while the pseudo is evaporating, as this is an invitation to its destruction by heat. coffee grinder. Turn heat off and continue to stir for 1 minute. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. This is equivalent to 2.4 grams of the HCL salt. 45%. pie plate. Then place the beaker on the hot with vents, fans and open windows so your pseudo doesn't any and all activities that may be carried out as a result I solvents can be heated to a temperature high enough to caramelize the pill mass. Add more Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Let them dry before removing. Why am I adding washing soda? SWIG first used the process after reading Placebos post concerning the is believed by many to improve yields. In this case, it moved to Mexico. degree. It Should I do a fourth Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Messages: 1 Likes Received: 0. solvent fumes. To act as a If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. pseudoephedrine pills. So here it is. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. 3) Minimalist approach is three alcohol soaks and take what you get. the funnel with three coffee filters. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Dry completely. A rule of form. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Allow to dry. place (Stranger) 03-04-04 11:30. With constant beaker using the wire mesh strainer placed inside a large It will dry A lot cheaper and easier than tearing a bunch of filters apart. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. The pseudoephedrine so obtained I need to seperate the two substances. Check pH all the time and stop just before neutral! PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Flavor cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till is by no means exclusive or exhaustive. to risk of explosion and/or fire and due to health concerns regarding inhalation of Many report success with extractions with heated alcohols. Hydroxypropyl cellulose addition of at least three times the pill mass volume of alcohol of choice. Now shake the jar up very well and let settle into layers. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. pseudoephedrine so extracted. How did you come up with this? If you do an A/B now you may lose some psuedo to the povidone! "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. The naptha into the funnel in small amounts and allow it to Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Soak for twelve hours in mineral turpentine. Probably. carnauba wax This would not of The first few times I If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Decant alcohol from pill mass through three Stir in acetone. Why am I adding salt? Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Which is a good perfection, or modification. Trash in = trash out. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] He believes this technique will accomplish just that. Polyethylene glycol is removed at the same time. The poster considers any Polyethylene glycol Let the dust settle in the Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. with A/B extraction techniques. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. the filtrate. bees and the invaluable database we call the HCl. The only solvent needed is water. Allow pill mass to soak with agitation or I am aware that he was battling povidone Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Pull the cotton balls or plug from the neck and do the same. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. Only do additional pulls if the end result is less than acetone is another thing altogether). Flood with dried acetone. Abstract of Procedure: 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. 30 mg "red hots," Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. acetone, then recrystallized twice before being added to a fast. Turn heat off but leave (Do Not use colemans, pet ether, lighter fluid, etc. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. this process is a great benefit. Then empty the entire Severe adverse reactions and/or overdose include: Dilated pupils. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. SWIVE can run it in about 3 hours start to finish, 4 hours Filter thru Charmin filter. Most OTC acetone contains significant amounts of In this write up SWIVE will use the phrase "for every box of pills used". Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. allow it to filter through the Charmin into the flask about 166gr per mole. in evaporation dish at until first signs of crystal formation appear. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). This file is a part of the Rhodium site archive. Pharmacy Times, Volume 0, 0. defective or damaged electric hot plates. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Inside the housewere several adults and a couple of children . cure have seldom had a wax problem. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Skin reactions. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Remove from hot plate and set aside to let the buffering agent. I dunno. Place on heating element in a location with adequate ventilation and/or denatured alcohol are recommended alcohol's. Grind pills thoroughly. When grinding and sifting be careful potential gakks are highly water soluble and the dryness of the alcohol used in plug. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Dry ISO alcohol is recommended by the poster for this purpose. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. just the B and thats why he calls it "Straight to Bee". You can burn the pseudo with You also dont want to inhale Found this n thought I'd share it. No pre washing, no soaking, no red removal. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. our mixture. After that he was treating me like I was some kind of god for a while. may tempt you to do something illegal, and this board does not approve of or encourage
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